How to identify the quality of gypsum powder?

1、測(cè)定結(jié)晶水含量

1. Determination of crystal water content

石膏粉是一種結(jié)晶混合物，其中會(huì)含有生石膏、半水石膏和無(wú)水石膏(過(guò)燒石膏）。在炒制過(guò)程中欠火夾生會(huì)出現(xiàn)生石膏,或者火大、炒制時(shí)間過(guò)長(zhǎng)造成過(guò)燒會(huì)出現(xiàn)無(wú)水石膏，這些都會(huì)影響石膏的凝結(jié)時(shí)間,影響生產(chǎn)的正常使用。有時(shí)由于石膏粉放置時(shí)間過(guò)長(zhǎng)受潮,也會(huì)影響正常使用。根據(jù)經(jīng)驗(yàn)和資料介紹,通過(guò)測(cè)定結(jié)晶水的含量，可判斷石膏粉質(zhì)量的好壞。一般合格的石膏粉結(jié)晶水的含量在4.5~5.5之間^若石膏粉的結(jié)晶水含量遠(yuǎn)低于此標(biāo)準(zhǔn)值,則說(shuō)明石膏粉過(guò)燒,注模時(shí)凝結(jié)時(shí)間太長(zhǎng)甚至不凝固;若石膏粉的結(jié)晶水含量遠(yuǎn)高于此標(biāo)準(zhǔn)值，則說(shuō)明石膏粉欠火或者受潮,注模時(shí)凝結(jié)時(shí)間短。以上兩種情況的石膏粉都不合格,在生產(chǎn)中不能使用。

Gypsum powder is a crystalline mixture containing raw gypsum, hemihydrate gypsum and anhydrous gypsum (overburned gypsum). In the process of frying, raw gypsum will appear when it is under fired, or anhydrous gypsum will appear when it is over fired due to high fire and too long frying time, which will affect the setting time of gypsum and the normal use of production. Sometimes the normal use will also be affected due to the moisture of gypsum powder due to too long storage time. According to the experience and data introduction, it can be judged by measuring the content of crystal water The quality of broken gypsum powder is good or bad. Generally, the content of qualified gypsum powder crystal water is between 4.5 ~ 5.5 ^ if the content of gypsum powder crystal water is far lower than this standard value, it indicates that the gypsum powder is over burned and the setting time is too long or even does not set during injection molding; if the content of gypsum powder crystal water is far higher than this standard value, it indicates that the gypsum powder is under fire or damp and the setting time is short during injection molding. The above two cases are different Gypsum powder is unqualified and cannot be used in production.

檢測(cè)石膏粉結(jié)晶水含量的方法是：準(zhǔn)確稱(chēng)取4(TC烘干后冷卻至室溫的試樣質(zhì)量G(—般為2?5g),放置于恒重的鉑金坩堝（或瓷坩堝）中，準(zhǔn)確稱(chēng)取其質(zhì)量為G1;在230±5°C下灼燒2h，取出移人干燥器內(nèi)，冷卻至室溫后稱(chēng)取其質(zhì)量為G2，則其結(jié)晶水百分含量為(Gt—G2)/GX100。

The method to detect the crystal water content of gypsum powder is as follows: accurately weigh the mass g of the sample cooled to room temperature after drying 4 (TC) (generally 2? 5g), place it in a platinum crucible (or porcelain crucible) with constant weight, and accurately weigh its mass as G1; burn it at 230 ± 5 ° C for 2h, take it out and transfer it into a dryer, cool it to room temperature, and weigh its mass as G2, then the percentage content of crystal water is (gt-g2) / gx100.

2、測(cè)定石膏粉的凝結(jié)時(shí)間

2. Determination of setting time of gypsum powder

凝結(jié)時(shí)間包括初凝時(shí)間和終凝時(shí)間。石膏粉凝結(jié)時(shí)間的質(zhì)量標(biāo)準(zhǔn)是：在標(biāo)準(zhǔn)稠度下，一般初凝時(shí)間不小于6min,終凝時(shí)間不大于25min。適宜的凝結(jié)時(shí)間是石膏粉在生產(chǎn)中正常使用的先決和必要的條件。初凝時(shí)間過(guò)短或終凝時(shí)間過(guò)長(zhǎng)都不合適。如果在使用中初凝時(shí)間太短，小于6min,則證明石膏粉沒(méi)有炒熟夾生，或受潮內(nèi)部含有生石裔，影響注模操作,表現(xiàn)為生產(chǎn)中注桶，耽誤生產(chǎn);若終凝時(shí)間太長(zhǎng)，遠(yuǎn)大于25tnin,則說(shuō)明石膏在炒制時(shí)過(guò)燒，里面含有過(guò)燒石膏，表現(xiàn)為注模時(shí)易漏漿,甚至石膏漿不凝固，影響生產(chǎn)。

The setting time includes the initial setting time and the final setting time. The quality standard of the setting time of gypsum powder is: under the standard consistency, the initial setting time is generally not less than 6min and the final setting time is not more than 25min. The appropriate setting time is the prerequisite and necessary condition for the normal use of gypsum powder in production. Too short initial setting time or too long final setting time is not appropriate. If the initial setting time is too short in use If the final setting time is too long, much more than 25 tnin, it indicates that the gypsum is over burned during frying and contains over burned gypsum, which is easy to leak slurry during molding, or even the gypsum slurry does not solidify, affecting the production.

這兩種情況的石膏粉在生產(chǎn)中都不能使用。故通過(guò)凝結(jié)時(shí)間的測(cè)定可判定石膏粉質(zhì)量的優(yōu)劣或者決定該石膏粉在生產(chǎn)中能否使用。

The gypsum powder in both cases can not be used in production. Therefore, the quality of gypsum powder can be determined by measuring the setting time, or whether the gypsum powder can be used in production.

3、從外觀上判斷

3. Judging from appearance

通過(guò)外觀上觀察和手感可初步判斷石膏粉質(zhì)量的優(yōu)劣。觀察就是看外觀包裝袋質(zhì)量情況和石膏粉的外觀顏色，手感就是用手搓一搓石膏粉的糙細(xì)程度(細(xì)度）。

The quality of gypsum powder can be preliminarily judged by appearance observation and hand feeling. Observation is to see the quality of appearance packaging bag and the appearance color of gypsum powder. Hand feeling is to rub the roughness (fineness) of gypsum powder by hand.

(1)若包裝塑料編織袋的材質(zhì)質(zhì)量差、松軟強(qiáng)度低、做工粗糙、編織稀疏(單位面積內(nèi)的經(jīng)緯數(shù)目不達(dá)標(biāo)）、顏色發(fā)灰綠黑色、內(nèi)部沒(méi)有防潮塑料袋、出現(xiàn)撒料現(xiàn)象、三無(wú)產(chǎn)品或外觀標(biāo)識(shí)(種類(lèi)名稱(chēng)、生產(chǎn)廠家、商標(biāo)、重量、聯(lián)系方式等）不齊全的石膏粉則很大可能不符合質(zhì)量標(biāo)準(zhǔn)、檔次質(zhì)量差，質(zhì)量穩(wěn)定性也不能保證。反之，那些包裝塑料編織袋用材好、做工精致、顏色發(fā)白、強(qiáng)度高、編織經(jīng)緯密集、內(nèi)部有防潮塑料袋、封口嚴(yán)密、外觀印刷清晰、標(biāo)識(shí)齊全、不撒料的石膏粉一般質(zhì)量較好、檔次高，質(zhì)量有保證。一般使用這種包裝袋的石裔粉白度高、細(xì)度細(xì)。若石膏粉是質(zhì)量上乘的、高附加值的高強(qiáng)度石膏粉、特種石膏粉(如母模石裔粉、原模石膏粉或樹(shù)脂石膏粉），其價(jià)格很高,是普通石膏粉的3?9倍。

(1) If the packaging plastic woven bag has poor material quality, low soft strength, rough workmanship, sparse weaving (the number of longitude and latitude per unit area does not meet the standard), gray green black color, no moisture-proof plastic bag inside, scattering phenomenon, and no product or appearance identification (type name, manufacturer, trademark, weight, contact information, etc.) incomplete gypsum powder may not meet the quality standards, poor grade quality, and quality stability can not be guaranteed. On the contrary, those packaging plastic woven bags have good materials, exquisite workmanship, white color, high strength, dense weaving longitude and weft, moisture-proof plastic bags inside, tight sealing, and clear appearance printing The gypsum powder with complete marks and no material spreading is generally of good quality, high grade and guaranteed quality. Generally, the stone powder in this packing bag has high whiteness and fine fineness. If the gypsum powder is high-strength gypsum powder and special gypsum powder with high quality and high added value (such as master mold stone powder, original mold gypsum powder or resin gypsum powder), its price is very high, which is 3-9 times that of ordinary gypsum powder.

(2)外觀上看，白度高的石膏粉細(xì)度目數(shù)高，質(zhì)量好，價(jià)格較高；而發(fā)灰發(fā)黑、里面有黑色雜質(zhì)的石膏粉質(zhì)量較差。用手的拇指和食指搓捻石膏粉,手感發(fā)沙粗糙的石膏粉細(xì)度糙，質(zhì)量較差、價(jià)格較低；而手感細(xì)膩的石音粉說(shuō)明細(xì)度細(xì)，質(zhì)量較好，價(jià)格也會(huì)較高。

(2) In appearance, the gypsum powder with high whiteness has high fineness, good quality and high price; while the gypsum powder with gray and black hair and black impurities inside is of poor quality. Rubbing and twisting the gypsum powder with the thumb and index finger of the hand, the gypsum powder with rough hand feel has rough fineness, poor quality and low price; while the stone sound powder with fine hand feel shows fine fineness, good quality and high price.

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